252 Atk Talonflame Acrobatics (110 BP) vs. 0 HP / 0 Def Mega Diancie: 60-72 (24.8 - 29.8%) -- 100% chance to 4HKO
+2 252 Atk Talonflame Acrobatics (110 BP) vs. 0 HP / 0 Def Mega Diancie: 120-142 (49.7 - 58.9%) -- 99.6% chance to 2HKO
32 Atk Mega Diancie Diamond Storm vs. 120 HP / 0 Def Talonflame: 880-1036 (269.1 - 316.8%) -- guaranteed OHKO
32 Atk Mega Diancie Diamond Storm vs. (Roost) 120 HP / 0 Def Talonflame: 440-518 (134.5 - 158.4%) -- guaranteed OHKO
Mega Diancie can switch rather freely into Talonflame and destroy it with a Diamond Storm, even after losing its Flying-type with Roost.
--
248 Atk Tough Claws Mega Aerodactyl Aqua Tail vs. 0 HP / 0 Def Mega Diancie: 248-292 (102.9 - 121.1%) -- guaranteed OHKO
32 Atk Mega Diancie Diamond Storm vs. 72 HP / 0 Def Mega Aerodactyl: 380-450 (119.1 - 141%) -- guaranteed OHKO
Mega Diancie may be able to OHKO Mega Aerodactyl... but so can Mega Aerodactyl! You should carefully avoid Aqua Tail, which can cleanly destroy Mega Diancie.
--
252 Atk Staraptor Close Combat vs. 0 HP / 0 Def Mega Diancie: 114-135 (47.3 - 56%) -- 80.9% chance to 2HKO
32 Atk Mega Diancie Diamond Storm vs. 0 HP / 4 Def Staraptor: 440-522 (141.4 - 167.8%) -- guaranteed OHKO
Mega Diancie is able tank a Close Combat and kill the bird with a single Diamond Storm.
--
0 SpA Clefable Moonblast vs. 0 HP / 0- SpD Mega Diancie: 102-120 (42.3 - 49.7%) -- guaranteed 3HKO
+1 0 SpA Clefable Moonblast vs. 0 HP / 0- SpD Mega Diancie: 151-178 (62.6 - 73.8%) -- guaranteed 2HKO
32 Atk Mega Diancie Diamond Storm vs. 252 HP / 172 Def Clefable: 174-205 (44.1 - 52%) -- guaranteed 3HKO after Leftovers recovery
Clefable can be quite difficult for Mega Diance to handle, since it can setup on her and heal damage with Soft-boiled. However, if you manage to switch Mega Diancie into a Thunder Wave then the moon fairy should be easier to handle, as long as it lacks Heal Bell.
--
252 Atk Life Orb Weavile Icicle Crash vs. 0 HP / 0 Def Mega Diancie: 157-187 (65.1 - 77.5%) -- guaranteed 2HKO
224 SpA Mega Diancie Moonblast vs. 0 HP / 0 SpD Weavile: 408-482 (145.1 - 171.5%) -- guaranteed OHKO
The best way to handle Weavile would be through revenge killing. Icicle Crash can take a chunk off of Mega Diancie's HP and finish her off with Ice Shard, so avoid to switch her in directly.
--
252+ SpA Life Orb Teravolt Kyurem-B Earth Power vs. 0 HP / 0- SpD Mega Diancie: 273-322 (113.2 - 133.6%) -- guaranteed OHKO
252+ SpA Teravolt Kyurem-B Earth Power vs. 0 HP / 0- SpD Mega Diancie: 210-248 (87.1 - 102.9%) -- 18.8% chance to OHKO
224 SpA Mega Diancie Moonblast vs. 0 HP / 0 SpD Kyurem-B: 390-458 (99.7 - 117.1%) -- 93.8% chance to OHKO
Kyurem-B could be a great gamble for Mega Diancie, but if you manage to Knock Off its Life Orb then you may stand a better chance.
--
252 SpA Mega Charizard Y Solar Beam vs. 0 HP / 0- SpD Mega Diancie: 312-368 (129.4 - 152.6%) -- guaranteed OHKO
32 Atk Mega Diancie Diamond Storm vs. 0 HP / 4 Def Mega Charizard Y: 808-952 (272 - 320.5%) -- guaranteed OHKO
Beware of Solar Beam! It isn't very healthy...
--
0 Atk Mega Altaria Earthquake vs. 0 HP / 0 Def Mega Diancie: 146-172 (60.5 - 71.3%) -- guaranteed 2HKO
+1 0 Atk Mega Altaria Earthquake vs. 0 HP / 0 Def Mega Diancie: 216-256 (89.6 - 106.2%) -- 37.5% chance to OHKO
224 SpA Mega Diancie Moonblast vs. 248 HP / 96 SpD Mega Altaria: 312-368 (88.3 - 104.2%) -- 31.3% chance to OHKO
Another risky match-up for Miss Diamond. Admittedly, this match-up relies a lot on luck, so Mega Diancie is a quite shaky check.
--
+1 0 SpA Mega Latias Stored Power (60 BP) vs. 0 HP / 0- SpD Mega Diancie: 133-157 (55.1 - 65.1%) -- guaranteed 2HKO
224 SpA Mega Diancie Moonblast vs. 248 HP / 0 SpD Mega Latias: 252-296 (69.4 - 81.5%) -- guaranteed 2HKO
224 SpA Mega Diancie Moonblast vs. +1 248 HP / 0 SpD Mega Latias: 168-200 (46.2 - 55%) -- 60.5% chance to 2HKO
As long as Mega Latias doesn't manage to setup, Mega Diancie is capable to handle the Eon without too many problems. Mega Diancie can even take a boosted Stored Power in a pinch, but must still beware.
--
252+ Atk Choice Band Dragonite Earthquake vs. 0 HP / 0 Def Mega Diancie: 340-400 (141 - 165.9%) -- guaranteed OHKO
252+ Atk Dragonite Earthquake vs. 0 HP / 0 Def Mega Diancie: 226-268 (93.7 - 111.2%) -- 62.5% chance to OHKO
+1 252+ Atk Dragonite Earthquake vs. 0 HP / 0 Def Mega Diancie: 340-400 (141 - 165.9%) -- guaranteed OHKO
224 SpA Mega Diancie Moonblast vs. 0 HP / 0 SpD Multiscale Dragonite: 178-210 (55.1 - 65%) -- guaranteed 2HKO
224 SpA Mega Diancie Moonblast vs. (No Multiscale) 0 HP / 0 SpD Dragonite: 356-420 (110.2 - 130%) -- guaranteed OHKO
Make sure to break the Multiscale ability before switching in Mega Diancie, otherwise you're in for a rough ride.
--
28 Atk Technician Mega Scizor Bullet Punch vs. 0 HP / 0 Def Mega Diancie: 348-412 (144.3 - 170.9%) -- guaranteed OHKO
224 SpA Mega Diancie Hidden Power Fire vs. 248 HP / 0 SpD Mega Scizor: 300-356 (87.4 - 103.7%) -- 25% chance to OHKO
Yikes! Mega Diancie simply doesn't want to meddle with this metallic bug! Handling Mega Scizor is extremely tricky and requires immense amounts of successful predictions to take it down, or a lucky Defense boost.
--
252 SpA Thundurus Thunderbolt vs. 0 HP / 0- SpD Mega Diancie: 147-174 (60.9 - 72.1%) -- guaranteed 2HKO
32 Atk Mega Diancie Diamond Storm vs. 0 HP / 4 Def Thundurus: 440-522 (147.1 - 174.5%) -- guaranteed OHKO
32 Atk Mega Diancie Diamond Storm vs. 0 HP / 4 Def Thundurus: 440-522 (147.1 - 174.5%) -- guaranteed OHKO
Mega Diancie can resist an unboosted Thunderbolt and strike back, but a powered-up Thundurus is a no-no for her. Facing him would require some good predictions.